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LADP-1A Sistimi ea Teko ea CW NMR - Mohlala o tsoetseng pele

Tlhaloso e Khutšoanyane:

Nuclear magnetic resonance (NMR) ke mofuta oa phetoho ea resonance e bakoang ke leqhubu la motlakase sebakeng se sa feleng sa khoheli.Ho tloha ha lithuto tsena li entsoe ka 1946, mekhoa le mekhoa ea nuclear magnetic resonance (NMR) li 'nile tsa ntlafatsoa ka potlako le ho sebelisoa haholo hobane li ka kena botebong ba ntho ntle le ho senya sampole,' me li na le melemo ea ho potlaka, ho nepahala le ho ba holimo. qeto.Matsatsing ana, ba kenelletse ho tloha ho fisiks ho ea k'hemistri, baeloji, jeoloji, kalafo ea bongaka, lisebelisoa le lithuto tse ling, ba bapala karolo e kholo lipatlisisong le tlhahisong ea mahlale.


Lintlha tsa Sehlahisoa

Li-tag tsa Sehlahisoa

 

Tlhaloso

Karolo ea boikhethelo: Metara ea khafetsa, karolo e itokiselitseng oscilloscope

Sistimi ena ea liteko ea continuous-wave nuclear magnetic resonance (CW-NMR) e na le makenete e phahameng ea homogeneity le yuniti e kholo ea mochini.Makenete oa ka ho sa feleng o sebelisoa ho fana ka matla a khoheli a mantlha a phahamisitsoeng ke sebaka se feto-fetohang sa motlakase, se hlahisoang ke li-coil, ho lumella phetoho e ntle ho matla a khoheli kaofela le ho lefella ho fetoha ha maemo a matla a khoheli a bakoang ke ho fapana ha mocheso.

Hobane ho hlokahala feela hona joale magnetizing e nyane bakeng sa sebaka se batlang se le tlase sa motlakase, bothata ba ho futhumatsa sistimi bo fokotsehile.Ka hona, sistimi e ka sebetsoa khafetsa ka lihora tse 'maloa.Ke sesebelisoa se loketseng sa liteko bakeng sa lilaboratori tse tsoetseng pele tsa fisiks.

Teko

1. Ho shebella ketsahalo ea nuclear magnetic resonance (NMR) ea hydrogen nuclei ka metsing le ho bapisa tšusumetso ea li-ion tsa paramagnetic;

2. Ho lekanya liparamente tsa hydrogen nuclei le fluorine nuclei, tse kang spin magnetic ratio, Lande g factor, joalo-joalo.

Litlhaloso

Tlhaloso

Tlhaloso

Khubu e lekantsoeng H le F
SNR > 46 dB (H-nuclei)
Maqhubu a oscillator 17 MHz ho 23 MHz, e feto-fetohang kamehla
Sebaka sa magnet pole Bophara: 100 mm;sebaka: 20 mm
Bophahamo ba lets'oao la NMR (ho fihla tlhorong) > 2 V (H-nuclei);> 200 mV (F-nuclei)
Homogeneity ea matla a khoheli molemo ho feta 8 ppm
Letoto la phetoho ea sebaka sa motlakase oa motlakase 60 Gauss
Palo ea maqhubu a coda > 15

 

 


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